10075-50-0
- Product Name：5-Bromoindole
- Molecular Formula：C8H6BrN
- Purity：99%
- Molecular Weight：264.33
Product Details
pd_meltingpoint:89-92 °C
Appearance:white to light brown powder or chunks
Manufacturer supply top purity 5-Bromoindole 10075-50-0 with ISO standards
- Molecular Formula:C8H6BrN
- Molecular Weight:264.33
- Appearance/Colour:white to light brown powder or chunks
- Vapor Pressure:0.000738mmHg at 25°C
- Melting Point:89-92 °C
- Refractive Index:1.711
- Boiling Point:316.9 °C at 760 mmHg
- PKA:16.04±0.30(Predicted)
- Flash Point:145.5 °C
- PSA：15.79000
- Density:1.66 g/cm3
- LogP:2.93040
5-Bromoindole(Cas 10075-50-0) Usage
|
Purification Methods |
Purify it by steam distillation from a faintly alkaline solution. Cool the aqueous distillate, collect the solid, dry it in a vacuum desiccator over P2O5 and recrystallise it from aqueous EtOH (35% EtOH) or pet ether/Et2O. UV in MeOH has at 279, 287 and 296nm (log 3.70, 3.69 and 3.53). The picrate has m 137-138o(dec) (from max Et2O/pet ether). [UV: Thesing et al. Chem Ber 95 2205 1962, UV and NMR: Lallemand & Bernath Bull Soc Chim Fr 4091 1970, Beilstein 20/7 V 36.] |
InChI:InChI=1/C8H6BrN/c9-7-1-2-8-6(5-7)3-4-10-8/h1-5,10H
10075-50-0 Relevant articles
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, p. 360 - 371 (2020)
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Dehydrogenation of indoline by cytochrome P450 enzymes: A novel "aromatase" process
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10075-50-0 Process route
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-
26807-69-2
N-acetylindololine-2-sulfonic acid sodium
-
-
10075-50-0
5-bromo-1H-indole
| Conditions | Yield |
|---|---|
|
N-acetylindololine-2-sulfonic acid sodium;
With
bromine;
In
water;
at 0 - 20 ℃;
for 2h;
With
sodium hydroxide;
In
water;
for 20h;
Reflux;
|
92% |
|
N-acetylindololine-2-sulfonic acid sodium;
With
bromine;
In
water;
at 0 - 20 ℃;
With
sodium hydroxide;
In
water;
for 20h;
Reflux;
|
92% |
|
With
bromine;
In
water;
at 0 - 5 ℃;
for 0.5h;
|
88% |
-
-
1196980-99-0
1-(5-bromo-1H-indol-1-yl)-2,2-dimethylpropan-1-one
-
-
10075-50-0
5-bromo-1H-indole
| Conditions | Yield |
|---|---|
|
With
water; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
tetrahydrofuran;
at 20 ℃;
for 24h;
|
99% |
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63843-81-2
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77248-65-8
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