1868106-31-3
- Product Name：tert-butyl 2-(hydroxymethyl)-7,8-dihydro-1,6-naphthyridine-6(5H)-carboxylate
- Molecular Formula：
- Purity：99%
- Molecular Weight：264.324
Product Details
Top Quality Chinese Manufacturer supply 1868106-31-3 tert-butyl 2-(hydroxymethyl)-7,8-dihydro-1,6-naphthyridine-6(5H)-carboxylate
- Molecular Formula:C14H20N2O3
- Molecular Weight:264.324
1868106-31-3 Relevant articles
PIPERIDINYL AMINE COMPOUNDS FOR THE TREATMENT OF AUTOIMMUNE DISEASE
-
Page/Page column 56-57, (2021/04/03)
The present invention relates to compoun...
HETEROCYCLIC CARBOXYLIC ACIDS AS ACTIVATORS OF SOLUBLE GUANYLATE CYCLASE
-
Paragraph 0486-0487, (2016/02/18)
The present invention relates to compoun...
1868106-31-3 Process route
-
-
259809-47-7
6-(tert-butoxycarbonyl)-2-methoxycarbonyl-5,6,7,8-tetrahydro-1,6-naphthyridine
-
-
1868106-31-3
tert-butyl 2-(hydroxymethyl)-7,8-dihydro-5H-1,6-naphthyridine-6-carboxylate
| Conditions | Yield |
|---|---|
|
With
diisobutylaluminium hydride;
In
tetrahydrofuran; toluene;
at 0 ℃;
for 2.5h;
|
0.459 g |
|
With
diisobutylaluminium hydride;
In
tetrahydrofuran;
at -70 - 25 ℃;
for 1.5h;
Inert atmosphere;
|
320 mg |
-
![2-chloro-7,8-dihydro-5H-[1,6]naphthyridine-6-carboxylic acid tert-butyl ester](/upload/2024/12/e71f2431-e404-4922-b644-6073412a920a.png)
-
1151665-15-4
2-chloro-7,8-dihydro-5H-[1,6]naphthyridine-6-carboxylic acid tert-butyl ester
-
-
1868106-31-3
tert-butyl 2-(hydroxymethyl)-7,8-dihydro-5H-1,6-naphthyridine-6-carboxylate
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 2 steps
1: palladium diacetate; 1,3-bis-(diphenylphosphino)propane; triethylamine / 16 h / 100 °C
2: diisobutylaluminium hydride / tetrahydrofuran / 1.5 h / -70 - 25 °C / Inert atmosphere
With
1,3-bis-(diphenylphosphino)propane; palladium diacetate; diisobutylaluminium hydride; triethylamine;
In
tetrahydrofuran;
|
1868106-31-3 Upstream products
-
259809-47-7
6-(tert-butoxycarbonyl)-2-methoxycarbonyl-5,6,7,8-tetrahydro-1,6-naphthyridine
-
1151665-15-4
2-chloro-7,8-dihydro-5H-[1,6]naphthyridine-6-carboxylic acid tert-butyl ester
Relevant Products
-
BENZYL N-(2-HYDROXYETHYL)CARBAMATECAS：77987-49-6
-
(S)-3-Hydroxypiperidine hydrochlorideCAS：475058-41-4
-
Methyl Ethyl KetoximeCAS：96-29-7
-
6-Cyano-2-naphtholCAS：52927-22-7
