4865-84-3
- Product Name：2-(1,2-Benzisoxazol-3-yl)acetic acid
- Molecular Formula：C9H7NO3
- Purity：99%
- Molecular Weight：177.159
Product Details
pd_meltingpoint:123 °C
Manufacturer supply good quality 2-(1,2-Benzisoxazol-3-yl)acetic acid 4865-84-3 with stock
- Molecular Formula:C9H7NO3
- Molecular Weight:177.159
- Vapor Pressure:2.3E-06mmHg at 25°C
- Melting Point:123 °C
- Boiling Point:377.3 °C at 760 mmHg
- PKA:3.60±0.30(Predicted)
- Flash Point:182 °C
- PSA：63.33000
- Density:1.394 g/cm3
- LogP:1.45490
2-(1,2-Benzisoxazol-3-yl)acetic acid(Cas 4865-84-3) Usage
InChI:InChI=1/C9H7NO3/c11-9(12)5-7-6-3-1-2-4-8(6)13-10-7/h1-4H,5H2,(H,11,12)/p-1
4865-84-3 Relevant articles
A PROCESS FOR THE MANUFACTURE OF ZONISAMIDE
-
Page/Page column 9, (2010/02/11)
The present invention describes an impro...
4865-84-3 Process route
-
![4-hydroxy[1]benzopyran-2-one](/upload/2024/12/264cb41e-aebb-41b9-88f2-e887b90ce3c1.png)
-
1076-38-6,92395-12-5
4-hydroxy[1]benzopyran-2-one
-
-
1196-29-8
2-hydroxyacetophenoneoxime
-
![2-(benzo[d]isoxazol-3-yl)acetic acid](/upload/2024/12/163bcdcb-afae-46e8-aae2-948516c678cb.png)
-
4865-84-3
2-(benzo[d]isoxazol-3-yl)acetic acid
Conditions
| Conditions | Yield |
|---|---|
|
With
methanol; hydroxylamine hydrochloride; sodium methylate;
for 5 - 10h;
Heating / reflux;
|
-
-
4865-84-3
2-(benzo[d]isoxazol-3-yl)acetic acid
-
-
73101-64-1
1,2-benzisoxazole-3-methanesulfonic acid sodium salt
Conditions
| Conditions | Yield |
|---|---|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid;
In
1,2-dichloro-ethane;
at 63 - 79 ℃;
for 1.5h;
With
sodium hydroxide;
In
water; 1,2-dichloro-ethane;
pH=>= 11;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid; Ethyl isobutyrate;
In
toluene;
at 80 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid; ethyl acetate;
In
dichloromethane; toluene;
at 70 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid; ethyl acetate;
In
chloroform; toluene;
at 70 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid; ethyl acetate;
In
toluene;
at 80 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid; N,N-dimethyl-formamide;
In
toluene;
at 80 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
1,4-dioxane; chlorosulfonic acid;
In
toluene;
at 80 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
1-methyl-pyrrolidin-2-one; chlorosulfonic acid;
In
toluene;
at 80 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid; acetonitrile;
In
1,2-dichloro-ethane; toluene;
at 70 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid; tert-butyl isocyanide;
In
1,2-dichloro-ethane; toluene;
at 70 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid; tert-butyl isocyanide;
In
toluene;
at 80 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid; Methyl pivalate;
In
toluene;
at 80 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid; benzonitrile;
In
toluene;
at 80 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid; Ethyl propionate;
In
toluene;
at 80 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid; benzoic acid ethyl ester;
In
toluene;
at 80 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid; monoethylene glycol diethyl ether;
In
toluene;
at 80 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid; 2,2-dimethyl-propanoic acid ethyl ester;
In
toluene;
at 80 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
|
|
2-(benzo[d]isoxazol-3-yl)acetic acid;
With
chlorosulfonic acid;
In
toluene;
at 80 ℃;
for 2h;
With
sodium hydroxide;
In
water;
pH=10;
Product distribution / selectivity;
|
4865-84-3 Upstream products
-
1076-38-6
4-hydroxy[1]benzopyran-2-one
4865-84-3 Downstream products
-
50471-23-3
1,2-benzisoxazole-3-acetaldehyde
-
37924-67-7
α-bromo-1,2-benzisoxazole-3-acetic acid
-
57148-90-0
2-(1,2-benzisoxazol-3-yl)ethanol
-
23008-68-6
2-(benzo[d]isoxazol-3-yl)acetamide
Relevant Products
-
1-Boc-3-PiperidinoneCAS：98977-36-7
-
1-Boc-4-CyanopiperidineCAS：91419-52-2
-
N-BOC-4-HydroxypiperidineCAS：109384-19-2
